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- W2564440521 abstract "Reliable and short synthetic routes to polycyclic aromatic hydrocarbons and nanographenes are important in materials science. Herein, we report an efficient one-step annulative π-extension reaction of alkynes that provides access to diarylphenanthrenes and related nanographene precursors. In the presence of a cationic palladium/o-chloranil catalyst system and dibenzosiloles or dibenzogermoles as π-extending agents, a variety of diarylacetylenes are transformed successfully into 9,10-diarylphenanthrenes in a single step with good functional-group tolerance. Furthermore, double π-extension reactions of 1,4-bis(phenylethynyl)benzene and diphenyl-1,3-butadiyne are demonstrated, affording oligoarylene products, which show potential for application in the synthesis of larger polycyclic aromatic hydrocarbons and nanographenes." @default.
- W2564440521 created "2017-01-06" @default.
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- W2564440521 date "2016-12-21" @default.
- W2564440521 modified "2023-09-30" @default.
- W2564440521 title "One‐Step Annulative π‐Extension of Alkynes with Dibenzosiloles or Dibenzogermoles by Palladium/ <i>o</i> ‐chloranil Catalysis" @default.
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- W2564440521 doi "https://doi.org/10.1002/anie.201610374" @default.
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