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• W2567663880 abstract "Tools that can effect electrophilic sulfur-promoted cation−π cyclizations are generally lacking, especially using alkylsulfide-based reagents. Herein we report that combining three different 1,2-dithioethers with Cl2 and SbCl5 generates isolable alkyldisulfanium salts that can effect such reactions. These new reagents can install −SMe, −SEt, and −SCH2CH2CF3 in modest, moderate, or good yield on diverse frameworks, including polyenes that terminate with electron-deficient groups. We also show that reagents such as dimethyl(methylthio)sulfonium tetrafluoroborate (DMTSF) can accomplish similar chemistry." @default.
• W2567663880 created "2017-01-06" @default.
• W2567663880 creator A5001052493 @default.
• W2567663880 creator A5079256239 @default.
• W2567663880 creator A5085302439 @default.
• W2567663880 date "2016-12-14" @default.
• W2567663880 modified "2023-10-13" @default.
• W2567663880 title "Alkyldisulfanium Salts: Isolable, Electrophilic Sulfur Reagents Competent for Polyene Cyclizations" @default.
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• W2567663880 doi "https://doi.org/10.1021/acs.orglett.6b02059" @default.
• W2567663880 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/27973855" @default.
• W2567663880 hasPublicationYear "2016" @default.
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