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- W2571006095 abstract "Deuteride phases in the zirconium-deuterium system in the temperature range 25-286$celsius$ have been studied in-situ by high resolution neutron diffraction. The study primarily focused on observations of $delta rightarrow gamma$ transformation at 180$celsius$, and the peritectoid reaction $alpha + delta leftrightarrow gamma$ at 255$celsius$ in commercial grade Zr powder that was deuterated to a deuterium/Zr ratio of one to one. A detailed description of the zirconium deuteride preparation route by high temperature gas loading is also described. The lattice parameters of $alpha$-Zr, $delta$-ZrD$_x$ and $epsilon$-ZrD$_x$ were determined by whole pattern crystal structure analysis, using Rietveld and Pawley refinements, and are in good agreement with values reported in the literature. The controversial $gamma$-hydride phase was observed both in-situ and ex-situ in deuterated Zr powder after a heat treatment at 286$celsius$ and slow cooling." @default.
- W2571006095 created "2017-01-13" @default.
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- W2571006095 date "2017-03-01" @default.
- W2571006095 modified "2023-09-27" @default.
- W2571006095 title "The preparation of Zr-deuteride and phase stability studies of the Zr-D system" @default.
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- W2571006095 doi "https://doi.org/10.1016/j.jnucmat.2017.01.008" @default.
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