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- W2571302606 abstract "This paper presents a multi‐residue method for direct enantioselective separation of chiral pharmacologically active compounds in environmental matrices. The method is based on chiral liquid chromatography and tandem mass spectrometry detection. Simultaneous chiral discrimination was achieved with a macrocyclic glycopeptide‐based column with antibiotic teicoplanin as a chiral selector working under reverse phase mode. For the first time, enantioresolution was reported for metabolites of ibuprofen: carboxyibuprofen and 2‐hydroxyibuprofen with this chiral stationary phase. Moreover, enantiomers of chloramphenicol, ibuprofen, ifosfamide, indoprofen, ketoprofen, naproxen and praziquantel were also resolved. The overall performance of the method was satisfactory in terms of linearity, precision, accuracy and limits of detection. The method was successfully applied for monitoring of pharmacologically active compounds at enantiomeric level in influent and effluent wastewater and in river water. In addition, the chiral recognition and analytical performance of the teicoplanin‐based column was critically compared with that of the α 1 ‐acid glycoprotein chiral stationary phase. Copyright © 2017 John Wiley & Sons, Ltd." @default.
- W2571302606 created "2017-01-13" @default.
- W2571302606 creator A5034486320 @default.
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- W2571302606 date "2017-01-31" @default.
- W2571302606 modified "2023-10-06" @default.
- W2571302606 title "Simultaneous enantiomeric analysis of pharmacologically active compounds in environmental samples by chiral LC-MS/MS with a macrocyclic antibiotic stationary phase" @default.
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- W2571302606 doi "https://doi.org/10.1002/jms.3904" @default.
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