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• W2572103665 abstract "Abstract Investigations of hydrothermal synthesis in the basic Na2O-Al2O3-SiO2-MnO4-H2O -system with variations of synthesis temperature and NaOH concentration were carried out. A permanganate bearing sodalite |Na7.7(1)(MnO4)1.7(2)(H2O)0.8(2)|[AlSiO4]6 could be obtained. The crystal structure and temperature-dependent behavior of this sodalite was examined by TG-DTA, in-situ temperature-dependent (TD) PXRD and Raman spectroscopy. Two phase transitions were observed: The first one at 600 K raises the symmetry from P 4 ¯ 3 n to P m 3 ¯ n due to the thermal expansion leading to a fully expanded framework. The second one at 900 K lowers the symmetry to P 23 , which is driven by the thermal decomposition reaction of the MnO4− ion, resulting in different fillings of the (nearest) neighboring cages forming a respective nosean type structure. The template-framework interactions were examined by temperature-dependent pre-resonance Raman spectroscopy and show the blocking of the template vibration through stronger template-framework interactions representing a solid state below ambient temperatures, whereas at elevated temperature the interaction strength decreases leading to a quasi-liquid single molecule template behavior." @default.
• W2572103665 created "2017-01-26" @default.
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• W2572103665 date "2017-04-01" @default.
• W2572103665 modified "2023-09-25" @default.
• W2572103665 title "Synthesis, temperature-dependent X-ray diffraction and Raman spectroscopic characterization of the sodalite to nosean phase-transformation of |Na 7.7(1) (MnO 4 ) 1.7(2) (H 2 O) 0.8(2) |[AlSiO 4 ] 6" @default.
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• W2572103665 doi "https://doi.org/10.1016/j.micromeso.2017.01.019" @default.
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