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- W2574001246 abstract "Abstract Alluaudites are promising electrochemical materials benefited from the open structure. Structural variations of alluaudites Na 2 M 3 (PO 4 ) 3 (M 3 =Fe 3 , Fe 2 Mn and FeMn 2 ) system have been studied by synchrotron radiation X-ray diffraction combined with diamond anvil cell technique up to ~10 GPa at room temperature. No phase transition is observed. The excellent structural stability is mainly due to the flexible framework plus strong covalent P-O bond. Mn 2+ instead of Fe can be described as Na + +2Fe 2+ →Mn 2+ +Fe 3+ +□ where □ represents a lattice vacancy. The replacement of Fe with larger Mn 2+ is equivalent to applying negative chemical pressure to the material. And it causes a more compressible b -axis, lattice expansion, structural compressibility and intensifies the core/electron-electron interactions of Fe. External pressure effect produces anisotropic lattice shrinkage. Structural considerations related to these variations and promising application prospects are discussed." @default.
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- W2574001246 date "2017-03-01" @default.
- W2574001246 modified "2023-09-23" @default.
- W2574001246 title "High pressure structural investigation on alluaudites Na 2 Fe 3 (PO 4 ) 3 -Na 2 FeMn 2 (PO 4 ) 3 system" @default.
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- W2574001246 doi "https://doi.org/10.1016/j.jssc.2017.01.007" @default.
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