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- W2576854059 abstract "建立了分子印迹固相萃取（MISPE）-超高效液相色谱-串联质谱（UPLC-MS/MS）同时测定鸡肉中9种氟喹诺酮药物残留的分析方法。样品经均质处理后，采用磷酸盐缓冲液提取，提取液经MISPE柱净化后，采用BEH C 18 柱分离，以乙腈-0.1%（v/v）甲酸水溶液为流动相，梯度洗脱，采用电喷雾正离子多反应监测模式，外标法定量。考察了MISPE柱对9种氟喹诺酮药物的吸附特异性；9种药物在0.25~100 μg/L范围内线性关系良好，相关系数（ r ）>0.9965；检出限和定量限分别为0.08 μg/kg和0.25 μg/kg；在0.25、2.5、5.0 μg/kg添加水平下，9种药物的回收率为65.8%~112.2%，批内、批间RSD分别为0.6%~13.5%和0.5%~14.9%；MISPE的最大柱容量为464.7~932.4 μg/L。该方法灵敏度好、操作简单、快速。" @default.
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- W2576854059 date "2016-01-01" @default.
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- W2576854059 title "Determination of nine fluoroquinolone residues in chicken by ultra performance liquid chromatography-tandem mass spectrometry coupled with molecularly imprinted solid phase extraction" @default.
- W2576854059 doi "https://doi.org/10.3724/sp.j.1123.2016.07024" @default.
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