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- W2579456380 abstract "We report a tunable library of N,N,N'-trisubstituted selenourea precursors and their reaction with lead oleate at 60-150 °C to form carboxylate-terminated PbSe nanocrystals in quantitative yields. Single exponential conversion kinetics can be tailored over 4 orders of magnitude by adjusting the selenourea structure. The wide range of conversion reactivity allows the extent of nucleation ([nanocrystal] = 4.6-56.7 μM) and the size following complete precursor conversion (d = 1.7-6.6 nm) to be controlled. Narrow size distributions (σ = 0.5-2%) are obtained whose spectral line widths are dominated (73-83%) by the intrinsic single particle spectral broadening, as observed using spectral hole burning measurements. The intrinsic broadening decreases with increasing size (fwhm = 320-65 meV, d = 1.6-4.4 nm) that derives from exciton fine structure and exciton-phonon coupling rather than broadening caused by the size distribution." @default.
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- W2579456380 date "2017-02-06" @default.
- W2579456380 modified "2023-10-10" @default.
- W2579456380 title "A Library of Selenourea Precursors to PbSe Nanocrystals with Size Distributions near the Homogeneous Limit" @default.
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- W2579456380 doi "https://doi.org/10.1021/jacs.6b11021" @default.
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