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• W2580451499 startingPage "228" @default.
• W2580451499 abstract "Crystallographic study was performed on the zinc undecanoate Zn(C11H21O2)2 by X-ray diffraction. Three polymorphs A, B and C were identified. The structures of A and B were solved from X-ray diffraction on platelets like single crystals obtained by crystallization in methanol. Polymorph A: SG = P21/c, a = 54.411(4) Å, b = 4.666(4) Å, c = 9.2231(8) Å, β = 92.54(7)°, V = 2341(2) Å3, Z = 4; polymorph B: SG = Cc, a = 53.451(2) Å, b = 4.707(1) Å, c = 9.178(1) Å, β = 91.53(7)°, V = 2308(2) Å3, Z = 4. Polymorph C has been detected in powder samples obtained by precipitation in aqueous solution. Its structure was solved from X-ray synchrotron diffraction data: SG = Pna21, a = 9.3386(6) Å, b = 4.7393(3) Å, c = 54.646(5) Å, V = 2418.5(3) Å3 and Z = 4. The three polymorphs have the usual layered structures encountered in zinc linear carboxylates series with Zn atoms in tetrahedral O-coordination. The forms A and C have the same building blocks but differ by their stacking. Two adjacent layers are 180° rotated around the short and the long axis in A and C respectively. The form B presents conformational disorder leading to modification of the preceding layers. In these form, the layers maintain the same orientation along the stacking direction." @default.
• W2580451499 created "2017-02-03" @default.
• W2580451499 creator A5000990984 @default.
• W2580451499 creator A5085338493 @default.
• W2580451499 date "2017-06-01" @default.
• W2580451499 modified "2023-10-09" @default.
• W2580451499 title "Polymorphism and polytypism in zinc aliphatic carboxylate: The complex case of Zn(C 11 H 21 O 2 ) 2" @default.
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• W2580451499 doi "https://doi.org/10.1016/j.matlet.2017.01.116" @default.
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