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• W2581126215 abstract "Abstract The cycloisomerization of readily available 2‐alkynylbenzamides has been conveniently carried out with CuCl 2 as catalyst under basic conditions in 1‐ethyl‐3‐methylimidazolium ethyl sulfate (EmimEtSO 4 ) as an unconventional solvent. The process leads to ( Z )‐3‐alkylideneisoindolin‐1‐ones in a chemo‐, regio‐, and stereoselective manner. The catalyst/solvent/base system could be recycled several times without appreciable loss of activity. The structures of representative products, that are, ( Z )‐3‐benzylidene‐2‐phenylisoindolin‐1‐one and ( Z )‐3‐pentylidene‐2‐phenylisoindolin‐1‐one, have been confirmed by X‐ray diffraction analysis, and DFT (density functional theory) calculations have been carried out to clarify the roles exerted by the base and CuCl 2 in favoring the reaction course leading to ( Z )‐3‐alkylideneisoindolinones." @default.
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• W2581126215 date "2017-01-23" @default.
• W2581126215 modified "2023-10-17" @default.
• W2581126215 title "Copper-Catalyzed Recyclable Synthesis of (<i>Z</i>)-3-Alkylideneisoindolinones by Cycloisomerization of 2-Alkynylbenzamides in Ionic Liquids" @default.
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• W2581126215 doi "https://doi.org/10.1002/slct.201601738" @default.
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