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- W2581681242 abstract "This chapter examines the thermally induced hydrogen release reactions and destruction products of hosting hydrogen storage materials in comparison to the behavior of sodium boronhydride (SB) and ammoniaborane (AB) carried out at temperatures up to 400°C. SB and AB contain 10.6 wt% and 19.6 wt% hydrogen, respectively, and are two of the most iinteresting hydrogen storage materials. SB and AB could be regarded as complexes of borane, X-BH3, constituted of Lewis base donor and borane Lewis acid. The identification of the reaction steps is of importance for an optimization of the hydrogen release. The thermal investigation of the pristine salts is a prerequisite in understanding the thermal behavior of the corresponding geopolymer-composites and the role played by the geopolymer framework. The dehydration is typically correlated with an endothermic peak with maximum at about 100°C. Using He as inert gas during the TG/DTA run and evacuating the sample before filling the He gas reveals mass losses of about 3-4 wt% for geopolymer samples of Si/Al ratios between 0.5 and 2.0. The oxidation of borohydride to cyclic metaborate is accompanied by H2 release, as evidenced by the TIR experiment of SB/KBr conducted in the presence of nitrate tracer (NaNO3)." @default.
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- W2581681242 date "2017-01-30" @default.
- W2581681242 modified "2023-10-14" @default.
- W2581681242 title "Investigations of the Thermally Induced Hydrogen Release of NaBh <sub>4</sub> , Nh <sub>3</sub> Bh <sub>3</sub> and Their Geopolymer Composites" @default.
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- W2581681242 doi "https://doi.org/10.1002/9781119321811.ch10" @default.
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