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- W2583901862 abstract "New organic ligands 3-(pyridine-2-yl)-4,5-dihydro-1H-pyrazole-1-thiocarboxamides (L) have been synthesized by a two or three step reaction sequence starting from substituted benzaldehydes and 2-acetyl pyridine. Copper(II) complexes with LCuCl2 composition were obtained by the reactions of these ligands with CuCl2·2H2O. The crystal structure of two synthesized complexes has been determined by X-ray analysis. Copper atoms located in a strongly distorted square piramidal environment and coordinated by pyrazoline and pyridine nitrogen atoms, thiocarbamoyl sulfur atom and two chloride-anions. All complexes undergo reversible or quasi-reversible electrochemical reduction at 0.45–0.28 V with the formation of Cu(I) containing intermediates. The cytotoxicity of copper containing complexes, comparable to cisplatin and doxorubicin, was demonstrated using cancer cell lines MCF-7, A549 and HEK293." @default.
- W2583901862 created "2017-02-10" @default.
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- W2583901862 date "2019-11-01" @default.
- W2583901862 modified "2023-09-23" @default.
- W2583901862 title "Synthesis of 3-(pyridine-2-yl)-4,5-dihydro-1H-pyrazole-1-thiocarboxamides and their copper(II) complexes" @default.
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- W2583901862 doi "https://doi.org/10.1016/j.arabjc.2017.01.005" @default.
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