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- W2586829994 abstract "Based on a thorough analysis of the sources of error in the iodometric determination of the oxygen deficiency ∂ in YBa2Cu3O7−δ, an improved procedure is given below. The crucial amendments to the methods originally published involve better control of the pH and a strict control of the sample dissolution steps. These improvements lead to an accuracy of better than ±0.01 in ∂ and show excellent correlation with data obtained from thermal analysis in a reducing atmosphere on a series of superconducting a nonsuperconducting ceramics exhibiting a large series of superconducting and nonsuperconducting ceramics exhibiting a large variation in oxygen. The thermal reduction process is discussed and the results are applied to an optimization of sintering conditions, using the oxygen content and relative densification of the material as a guideline." @default.
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- W2586829994 date "1992-01-01" @default.
- W2586829994 modified "2023-09-26" @default.
- W2586829994 title "Study of sintering characteristics using an improved method for the determination of the oxygen content in YBa2Cu3O7−δ" @default.
- W2586829994 doi "https://doi.org/10.1063/1.42085" @default.
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