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- W2588451936 abstract "We found that dichloromethane is a powerful chlorinating reagent for the congested 3° and 2° Csp3–Br bond of α-bromocarbonyl amides, esters, and ketones. In the presence of an appropriate copper complex as a catalyst, the desired chlorination occurred within an hour. Control experiments revealed that in situ-generated CuCl2 is a key chlorinating agent that reacts with the 3° or 2° alkyl radicals generated by the reaction between an α-bromocarbonyl compound and a Cu(I) salt." @default.
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- W2588451936 date "2017-05-05" @default.
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- W2588451936 title "Dichloromethane as a Chlorination Reagent for α-Bromocarbonyl Compounds in the Presence of a Copper Catalyst" @default.
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- W2588451936 doi "https://doi.org/10.1246/cl.170062" @default.
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