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• W2588491100 endingPage "247" @default.
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• W2588491100 abstract "Copper(II) complexation reactions with neutral N-donor ligands (Bipy, Phen, NH3) in the presence of the bulky decachloro-closo-decaborate dianion were studied. Copper(II) complexes can be prepared from copper(II) salts or copper(I) salts by redox reactions proceeding in air. The complexes [Cu(Bipy)3][B10Cl10]·2CH3CN (1·2CH3CN), [Cu(Bipy)3][B10Cl10]·2Bipy (1·2Bipy), [Cu(Bipy)2Cl]2[B10Cl10]·2DMF (2·2DMF), [Cu(Phen)2Cl]2[B10Cl10]·DMSO·1.25H2O (3·DMSO·1.25H2O) and [Cu(NH3)4(CH3CN)2][B10Cl10] (4) were prepared and characterized by X-ray diffraction as well as IR and 11B NMR spectroscopies. Complexes 1·2CH3CN, 2·2DMF, and 4 were also studied using 35Cl NQR spectroscopy. Secondary interactions were selected from all the interatomic contacts found in these crystals by X-ray diffraction. Hydrogen N–H⋯Cl–B, C–H⋯Cl–B and p⋯π (B–Cl⋯C) secondary bonds were identified in all the compounds, the spectroscopic data being generally in accordance with the results of the X-ray diffraction." @default.
• W2588491100 created "2017-02-24" @default.
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• W2588491100 date "2017-05-01" @default.
• W2588491100 modified "2023-10-01" @default.
• W2588491100 title "Decachloro-closo-decaborate anion in copper(II) complexation reactions with N-donor ligands: 35Cl NQR and X-ray studies" @default.
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• W2588491100 doi "https://doi.org/10.1016/j.poly.2017.02.015" @default.
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