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- W2589682810 abstract "Abstract Residual hydrogen (H 2 ) gas in the analysis chamber of an atom probe instrument limits the ability to measure H concentration in metals and alloys. Measuring H concentration would permit quantification of important physical phenomena, such as hydrogen embrittlement, corrosion, hydrogen trapping, and grain boundary segregation. Increased insight into the behavior of residual H 2 gas on the specimen tip surface in atom probe instruments could help reduce these limitations. The influence of user-selected experimental parameters on the field adsorption and desorption of residual H 2 gas on nominally pure copper (Cu) was studied during ultraviolet pulsed laser atom probe tomography. The results indicate that the total residual hydrogen concentration, H TOT , in the mass spectra exhibits a generally decreasing trend with increasing laser pulse energy and increasing laser pulse frequency. Second-order interaction effects are also important. The pulse energy has the greatest influence on the quantity H TOT , which is consistently less than 0.1 at.% at a value of 80 pJ." @default.
- W2589682810 created "2017-03-03" @default.
- W2589682810 creator A5022995015 @default.
- W2589682810 date "2017-02-22" @default.
- W2589682810 modified "2023-09-27" @default.
- W2589682810 title "Controlling residual hydrogen gas in mass spectra during pulsed laser atom probe tomography" @default.
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- W2589682810 doi "https://doi.org/10.1186/s40679-017-0043-4" @default.
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