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• W2590372577 abstract "Reactions of [8-HCCCH2O-8′-I-3,3′-Co(1,2-C2B9H10)2]- ([2]Cs) with 5-iodo-2’-deoxyuridine under Sonogashira reaction conditions resulted in a cobalt bis(1,2-dicarbollide)(-I) 5-ethynyl-2'-deoxyuridine conjugate ([3]Cs) linked via short spacer. Its intramolecular cyclization led to furo [2,3-d]pyrimidin-2(3H)-one isomer ([4]Cs). Compounds [3]Cs and [4]Cs demonstrated moderate cytotoxicity, however they did not have antiviral activity against the viruses tested. A new terminal charge-compensated cobalt bis(1,2-dicarbollide)(-I) derivative with terminal alkyne group (5) was synthesized from 8,8’-μ-I-3,3′-Co(1,2-C2B9H10)2 and dimethylpropargyl amine. It was found that contrary to [2]Cs compound 5 did not react with 5-iodo-2’-deoxyuridine under Sonogashira reaction conditions. Total electrostatic potential (TEP) calculations gave explanation of this phenomenon." @default.
• W2590372577 created "2017-03-03" @default.
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• W2590372577 date "2017-11-01" @default.
• W2590372577 modified "2023-10-06" @default.
• W2590372577 title "Disubstituted cobalt bis(1,2-dicarbollide)(-I) terminal alkynes: Synthesis, reactivity in the Sonogashira reaction and application in the synthesis of cobalt bis(1,2-dicarbollide)(-I) nucleoside conjugates" @default.
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• W2590372577 doi "https://doi.org/10.1016/j.jorganchem.2017.02.030" @default.
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