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• W2591627655 abstract "Abstract A combination of electrochemical methods, X-ray photoelectron spectroscopy and current-sensing atomic force microscopy has been used to study the anodic reactivity of close-to-stoichiometric UO 2.002 , SIMFUEL, and Gd and Dy-doped UO 2 . Experiments were conducted in 0.1 mol L −1 NaCl solutions containing either bicarbonate/carbonate or phosphate at pH = 10. Anodic oxidation of the UO 2 matrix and its dissolution were both suppressed by doping, with the reactivities being in the order UO 2.002  > SIMFUEL > Gd-doped UO 2  > Dy-doped UO 2 . The onset of dissolution for SIMFUEL and the doped specimens was initiated by tetragonal distortions of the cubic matrix and was accompanied by a deeper more extensive oxidation of the UO 2 matrix. The composition of the surface of UO 2.002 was non-uniform, leading to the sub-thermodynamic oxidation and dissolution of more non-stoichiometric locations. Oxidation of the matrix was suppressed in phosphate solution and the onset of oxidation to U VI led to the formation of a protective uranyl phosphate layer. By contrast, in bicarbonate/carbonate solutions, U VI species were complexed by carbonate and dissolved." @default.
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• W2591627655 date "2017-05-01" @default.
• W2591627655 modified "2023-09-30" @default.
• W2591627655 title "The Electrochemical Study of Dy2O3 Doped UO2 in Slightly Alkaline Sodium Carbonate/bicarbonate and Phosphate Solutions" @default.
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• W2591627655 doi "https://doi.org/10.1016/j.electacta.2017.03.075" @default.
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