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- W2593422918 abstract "A phosphino-imidazoline (PHIM) ligand possessing axial chirality is prepared in a straightforward five-step synthesis. Configurational stability around the chiral axis is achieved by the diastereofacial π-stacking between the pentafluorophenyl and the naphthalene rings. In particular, access to enantiopure ligand (S,S,Ra)-2a was realized by fractional crystallization of the corresponding ∼3:1 atropdiastereomeric mixture. The preliminary application of ligand (S,S,Ra)-UCD-PHIM showed excellent activities in the enantioselective copper-catalyzed A3 coupling (ee’s up to 98.1% and yields up to 98%)." @default.
- W2593422918 created "2017-03-16" @default.
- W2593422918 creator A5021761166 @default.
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- W2593422918 date "2017-02-27" @default.
- W2593422918 modified "2023-10-18" @default.
- W2593422918 title "Diastereofacial π-Stacking as an Approach To Access an Axially Chiral P,N-Ligand for Asymmetric Catalysis" @default.
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- W2593422918 doi "https://doi.org/10.1021/acscatal.6b03427" @default.
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