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- W2595231388 abstract "The technique described in this presentation allows detectionof metal nanoparticles and quantum dots (QDs) injected on thesilica gel spread on aluminum foil or filtration paper. Themodified laser system UP-266 MACRO equipped with softwarecontrolled stages in x and y directions was used. The preparedsubstrates with injected nanoparticles were placed into alab-made holder. Pulse energy was set to 10 mJ while plasmaemission was collected and transported by means of a 3 m longoptical fiber into the entrance of a monochromator (Jobin Yvon,TRIAX 320) and detected with the ICCD detector (Princeton, PIMAX 3). The raster covered 15 × 15 points with spacing 500 umwhile laser spot diameter was approximately 100 um. In doublepulse configuration (DP LIBS) the second, re-heating lasersystem, that propagates beam parallel to the sample surface wasused Q-Smart Nd:YAG laser at fundamental wavelength 1064 nm andenergy 100 mJ per pulse. This laser was focused by 80 mm focallength glass lens to intersect the path of the first laser beamand finally to create a coincident spark about 0.5 mm above thesample surface. Both configurations were employed forinvestigation of different types of metal-based nanoparticlesafter injection of different volumes and differentconcentrations on to filtration paper and silica gel spread onaluminum foil. Special attention was paid to study of QDscontaining CdS, CdTe, CdSe (or their combinations) stabilizedwith glutathione (GSH), cysteine (Cys), mercaptosuccinic acid(MSA) or aminoethanethiol. The feasibility of their 2Ddistribution mapping on the substrate by LIBS was examined inconnection with the separation (or preconcentration)possibilities." @default.
- W2595231388 created "2017-03-23" @default.
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- W2595231388 date "2016-01-18" @default.
- W2595231388 modified "2023-09-26" @default.
- W2595231388 title "Laser-Induced Breakdown Spectroscopy 2D Distribution Mapping ofNanoparticles" @default.
- W2595231388 hasPublicationYear "2016" @default.
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