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• W2596079187 abstract "Abstract Preparation of uniform, spherical Li 4 Ti 5 O 12 with high tap density is significant to achieve a high volumetric energy density in lithium‐ion batteries. Herein, Li 4 Ti 5 O 12 microspheres with variable tap density and tunable size distribution were synthesized by a newly designed industrial spray‐drying approach. The slurry concentration, sintering time, sintering conditions after spraying, and the effect of lithium/titanium molar ratio on the lithium‐ion (Li + ) storage capability were investigated. A narrow particle size distribution of around 10 μm and a high tap density close to 1.4 g cm −3 of the Li 4 Ti 5 O 12 spheres can be obtained under the optimized conditions. The Li 4 Ti 5 O 12 spheres can deliver a much higher capacity of 168 mAh g −1 at a rate of 1 C and show a high capacity retention of 97.7 % over 400 cycles. The synthetic conditions are confirmed to be critical for improving the electron conductivity and Li + diffusivity by adjusting the crystal and spatial structures. As‐prepared high‐performance Li 4 Ti 5 O 12 is an ideal electrode for lithium‐ion batteries or capacitors; meanwhile, the presented approach is also applicable for preparing other kind of spherical materials." @default.
• W2596079187 created "2017-03-23" @default.
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• W2596079187 date "2017-05-29" @default.
• W2596079187 modified "2023-10-16" @default.
• W2596079187 title "High Tap Density Li₄Ti₅O₁₂Microspheres: Synthetic Conditions and Advanced Electrochemical Performance" @default.
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• W2596079187 doi "https://doi.org/10.1002/ente.201700069" @default.
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