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• W2597157068 abstract "Abstract Nanometric-sized gadolinia (Gd 2 O 3 ) powders were obtained by applying solid-state displacement reaction at room temperature and low temperature calcination. The XRD analysis revealed that the room temperature product was gadolinium hydroxide, Gd(OH) 3 . In order to induce crystallization of Gd 2 O 3 , the subsequent calcination at 600 ∼ 1200 °C of the room temperature reaction products was studied. Calculation of average crystallite size ( D ) as well as separation of the effect of crystallite size and strain of nanocrystals was performed on the basic of Williamson-Hall plots. The morphologies of powders calcined at different temperatures were followed by scanning electron microscopy. The pure cubic Gd 2 O 3 phase was made at 600 °C which converted to monoclinic Gd 2 O 3 phase between 1400° and 1600 °C. High-density (96% of theoretical density) ceramic pellet free of any additives was obtained after pressureless sintering at 1600 °C for 4 h in air, using calcined powder at 600 °C." @default.
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• W2597157068 date "2017-07-01" @default.
• W2597157068 modified "2023-10-15" @default.
• W2597157068 title "Synthesis and characterization of nanometric gadolinia powders by room temperature solid-state displacement reaction and low temperature calcination" @default.
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• W2597157068 doi "https://doi.org/10.1016/j.jeurceramsoc.2017.03.004" @default.
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