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- W2597713456 abstract "Phthalides have been easily prepared by the treatment of methyl o-iodobenzoates with a silylmethyl Grignard reagent in the presence of ketones. The electron-withdrawing ester moiety of methyl o-iodobenzoates and the low nucleophilicity of the silylmethyl Grignard reagent prompted a smooth iodine–magnesium exchange reaction, at room temperature, without affecting the ester moiety or resulting in an undesired reaction with electrophilic ketones. This simple method, wherein special control of the reaction temperature was unnecessary, has allowed the synthesis of various phthalides, including a phenolphthalein derivative." @default.
- W2597713456 created "2017-04-07" @default.
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- W2597713456 date "2017-06-05" @default.
- W2597713456 modified "2023-09-25" @default.
- W2597713456 title "Facile Synthesis of Phthalides from Methyl ortho-Iodobenzoates and Ketones via an Iodine–Magnesium Exchange Reaction Using a Silylmethyl Grignard Reagent" @default.
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- W2597713456 doi "https://doi.org/10.1246/cl.170211" @default.
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