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- W2600717483 abstract "Nitridosilicates represent an intriguing class of materials and are typically made up of highly condensed tetrahedral network structures. Alkaline-earth nitridosilicates emerged as unique host materials for Eu2+ doped luminophores which found broad application in phosphor-converted (pc)-LEDs. In contrast to common strategies of preparing nitridosilicates by bottom-up syntheses, we have now succeeded to post-synthetically design nitridosilicates by ion exchange in metal halide melts. We describe the syntheses of hitherto unknown but predicted alkaline-earth nitridosilicates, Mg2Si5N8 and β-Ca2Si5N8. Both compounds were obtained by ion exchange starting from pre-synthesized nitridosilicates. In situ investigations of the ion-exchange process show that the Si–N network topology remains preserved. Therefore the reaction offers a significant increase of synthetic control with respect to classical bottom-up syntheses." @default.
- W2600717483 created "2017-04-07" @default.
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- W2600717483 date "2017-03-27" @default.
- W2600717483 modified "2023-10-01" @default.
- W2600717483 title "Increased Synthetic Control-Gaining Access to Predicted Mg2 Si5 N8 and β-Ca2 Si5 N8" @default.
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- W2600717483 doi "https://doi.org/10.1002/anie.201701361" @default.
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