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• W2601527730 abstract "Solvent-free copolymerization of epoxides derived from fatty esters of waste cooking oil with phthalic anhydride using (salen)CrIIICl as catalyst and n-Bu4NCl/DMAP (tetrabutylammonium chloride/4-(dimethylamino)pyridine) as co-catalysts was carried out for the first time under microwave irradiation, where reaction time was reduced from a number of hours to minutes. The polyesters were obtained with molecular weight (Mw = 3100–6750 g/mol) and dispersity values (D = 1.18–1.92) when (salen)CrIIICl/n-Bu4NCl was used as catalysts. Moreover, in the case of DMAP as a co-catalyst, polyesters with improved molecular weight (Mw = 5500–6950 g/mol) and narrow dispersity values (D = 1.07–1.28) were obtained even at reduced concentrations of (salen)CrIIICl and DMAP. The obtained products were characterized and evaluated by attenuated total reflection-Fourier transform infrared spectroscopy (ATR-FTIR), proton nuclear magnetic resonance (1H-NMR) spectroscopy, gel permeation chromatography (GPC), thermogravimetric analysis (TGA) and differential scanning calorimetric (DSC) Techniques." @default.
• W2601527730 created "2017-04-07" @default.
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• W2601527730 date "2017-03-20" @default.
• W2601527730 modified "2023-09-24" @default.
• W2601527730 title "Microwave-Assisted Catalytic Synthesis of Bio-Based Copolymers from Waste Cooking Oil" @default.
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• W2601527730 doi "https://doi.org/10.3390/ma10030315" @default.
• W2601527730 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/5503379" @default.
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