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• W2602423948 abstract "Abstract Porous magnesium-aluminium layered double hydroxides (LDH) were prepared through intercalation and decomposition of hydrogen peroxide (H 2 O 2 ). This process generates oxygen gas nano-bubbles that pierce holes in the layered structure of the material by local pressure build-up. The decomposition of the peroxide can be triggered by microwave radiation or chemically by reaction with iodide (I − ) ions. The carbonate LDH version [Mg 0.80 Al 0.20 (OH) 2 ](CO 3 ) 0.1 ∙mH 2 O was synthesized by microwave-assisted urea coprecipitation and further modified by iodide or H 2 O 2 intercalation. High resolution Scanning Electron Microscopy (HR-SEM) and Brunauer-Emmet-Teller (BET) analysis were used to assess the morphology and surface area of the new porous materials. The presence of H 2 O 2 in the interlayer region and later decomposition triggered by microwave radiation generated more pores on the surface of the LDH platelets, increasing their specific surface area from initially 9 m 2 /g to a maximum of 67 m 2 /g. X-Ray Diffraction showed that the formation of the pores did not affect the remaining crystal structure, allowing possible further functionalization of the material." @default.
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• W2602423948 date "2017-03-28" @default.
• W2602423948 modified "2023-09-27" @default.
• W2602423948 title "Porous Layered Double Hydroxides Synthesized using Oxygen Generated by Decomposition of Hydrogen Peroxide" @default.
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• W2602423948 doi "https://doi.org/10.1038/s41598-017-00283-9" @default.
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