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• W2602447327 abstract "A highly efficient, selective, and rapid transformation of primary amines and diamines to isothiocyanates and cyclic thioureas is disclosed. As opposed to established approaches that employ toxic or volatile electrophilic liquids and require reaction control (i.e., slow addition, cooling), this protocol utilizes the bench-stable, solid reagent (Me4N)SCF3 at room temperature. The method is characterized by operational simplicity, high speed, efficiency, high functional group tolerance, and late-stage applicability. The byproducts are solids, allowing isolation of the target compounds by filtration." @default.
• W2602447327 created "2017-04-07" @default.
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• W2602447327 date "2017-03-30" @default.
• W2602447327 modified "2023-10-13" @default.
• W2602447327 title "Synthesis of Isothiocyanates and Unsymmetrical Thioureas with the Bench-Stable Solid Reagent (Me₄N)SCF₃" @default.
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• W2602447327 doi "https://doi.org/10.1021/acs.orglett.7b00689" @default.
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