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- W2603671374 abstract "A highly convergent total synthesis of (+)-methynolide, based on two types of stereoselective aldol reaction, was achieved. The C1-C8 and C9-C11 fragments of (+)-methynolide were prepared by a vinylogous Mukaiyama aldol reaction using a vinyl ketene silyl N,O-acetal, and a Ti-mediated aldol reaction of a lactyl-bearing chiral oxazolidin-2-one, respectively. Yamaguchi esterification of both fragments and ring-closing metathesis afforded (+)-methynolide." @default.
- W2603671374 created "2017-04-07" @default.
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- W2603671374 date "2017-06-01" @default.
- W2603671374 modified "2023-10-09" @default.
- W2603671374 title "Total synthesis of (+)-methynolide using a Ti-mediated aldol reaction of a lactyl-bearing oxazolidin-2-one, and a vinylogous Mukaiyama aldol reaction" @default.
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- W2603671374 doi "https://doi.org/10.1016/j.tet.2017.03.093" @default.
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