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• W2604036900 abstract "We report the nitration of tris(hydroxymethyl)aminomethane to tris(nitromethyl)-aminomethane (2) and its corresponding hydrogen chloride (3) and hydrogen bromide (4) salts. While both 3 and 4 conglomerate into tetramers, there are significant differences in the packing of those tetrameric units. In both 3 and 4 the tetrameric units arrange in a hexagonal pattern, but in 3 the units adopt alternating orientations leading to severe interlocking of the alkyl nitrate groups. This ultimately leads to a 2-fold decrease in the mechanical sensitivity of 4 relative to 3 and suggests that utilizing anion size may lead to more efficient packing arrangements and reduced mechanical sensitivity in energetic salts." @default.
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• W2604036900 date "2017-04-26" @default.
• W2604036900 modified "2023-09-25" @default.
• W2604036900 title "Reduction of Mechanical Sensitivity in Alkyl Nitrate Explosives through Efficient Crystal Packing" @default.
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• W2604036900 doi "https://doi.org/10.1021/acs.cgd.7b00159" @default.
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