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• W2605486041 abstract "AbstractRare-earth complexes of the general formula [Ln(H2L1)2(NO3)3] [Ln = Gd (1), Ho (2) or Nd (3)] were prepared from an o-vanillin derived Schiff base ligand, 2-((E)-(1-hydroxy-2-methylpropan-2-ylimino)methyl)-6-methoxyphenol (H2L1). The single-crystal X-ray diffraction studies and SHAPE analyses of the Gd(III) and Ho(III) complexes show that the complexes are ten-coordinate and exhibit distorted tetradecahedron geometries. The phenolate oxygen-bridged dinuclear complex, [Ce2(H2L1)(ovan)3(NO3)3] (4, ovan = monodeprotonated o-vanillin), was obtained from the reaction of Ce(NO3)3∙6H2O with H2L1. X-ray analysis revealed that hydrolysis of H2L1 occurred to yield o-vanillin, which bridged two cerium atoms with the Ce⋯Ce distance equal to 3.8232(6) A. The Ce(III) ions are both ten-coordinate, but have different coordination environments, showing tetradecahedron and staggered dodecahedron geometries, respectively. With proton migration occurring from the phenol group to the imine function, complexation of th..." @default.
• W2605486041 created "2017-04-28" @default.
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• W2605486041 date "2017-04-26" @default.
• W2605486041 modified "2023-09-23" @default.
• W2605486041 title "Synthesis and characterization of lanthanide complexes prepared with 2-((E)-(1-hydroxy-2-methylpropan-2-ylimino)methyl)-6-methoxyphenol" @default.
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• W2605486041 doi "https://doi.org/10.1080/00958972.2017.1319568" @default.
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