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- W2605693145 abstract "Abstract In a strong acidic environment, ordered earthworm‐like mesoporous silica has been synthesized with CTAB templating and fluoride ion (F − ) as a counterion. The synthesized products were characterized by small‐angle X‐ray diffraction ( SXRD ), scanning electron microscopy ( SEM ), transmission electron microscopy ( TEM ), N 2 adsorption‐desorption isotherms, and Fourier‐transform infrared spectroscopy ( FTIR ). The effects of F/Si mole ratio on the morphology, surface area, and the pore size of the sample were discussed. It was found that a F/Si mole ratio at 0.083 induced the formation of 3D hexagonal mesophase, whereas higher F/Si mole ratios led to the formation of 2D hexagonal mesoporous silica, the optimum molar ratio of F/Si for the formation of delicate earthworm‐like mesoporous silica was observed at 0.250. The effects of the F/Si mole ratio, surfactant chain length, acid concentration, and shear flow on morphology were also studied." @default.
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- W2605693145 date "2017-04-10" @default.
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- W2605693145 title "Effects of fluoride ion on the formation of earthworm-like mesoporous silica" @default.
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- W2605693145 doi "https://doi.org/10.1111/jace.14696" @default.
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