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- W2606369878 abstract "Procaine hydrochlorate is identified by the melting point of Procaine picrate (JP XII). Although the melting points of monopicrate (1) and dipicrates (2) of procaine have been reported, they are inconsistent each other in their reports. It is not specified 1 or 2 in JP XII. From these reasons, the crystal structures of 1 and 2 of procaine have been elucidated by X-ray crystallographic analysis and each melting point is clarified. 1 is formed through the hydrogen bond between the phenolic hydroxyl group of a picric acid molecule and the tertiary amine of a procaine molecule, and the melting point of 1 was 133-135°C (decomp.). 2 is formed through the hydrogen bonds between the tertiary and the first amines of a procaine molecule and the phenolic hydroxyl groups of two picric acid molecules, respectively. The melting point of 2 was 152-155°C (decomp.)." @default.
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- W2606369878 date "1994-01-01" @default.
- W2606369878 modified "2023-09-27" @default.
- W2606369878 title "The Crystal Structures of Monopicrate and Dipicrates of Procaine" @default.
- W2606369878 doi "https://doi.org/10.1248/yakushi1947.114.1_21" @default.
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