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• W2606973023 abstract "Stereoselective high-performance liquid chromatographic and subcritical fluid chromatographic separations of 19 Nα -Fmoc proteinogenic amino acid enantiomers were carried out by using Quinidine-based zwitterionic and anion-exchanger-type chiral stationary phases Chiralpak ZWIX(-) and QD-AX. For optimization of retention and enantioselectivity, the ratio of bulk solvent components (MeOH/MeCN, H2 O/MeOH, or CO2 /MeOH) and the nature and concentration of the acid and base additives (counter- and co-ions) were systematically varied. The effect of column temperature on the enantioseparation was investigated and thermodynamic parameters were calculated from the van't Hoff plots ln α vs. 1/T. The thermodynamic parameters revealed that the enantioseparations were enthalpy-driven. The elution sequence was determined in all cases and with the exception of Fmoc-Cys(Trt)-OH, it was identical on both chiral stationary phases whereby the L-enantiomers eluted before the D-enantiomers." @default.
• W2606973023 created "2017-04-28" @default.
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• W2606973023 date "2017-04-19" @default.
• W2606973023 modified "2023-10-16" @default.
• W2606973023 title "Liquid and subcritical fluid chromatographic enantioseparation of <i>N</i> ^α -Fmoc proteinogenic amino acids on <i>Quinidine</i> -based zwitterionic and anion-exchanger type chiral stationary phases. A comparative study" @default.
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• W2606973023 doi "https://doi.org/10.1002/chir.22700" @default.
• W2606973023 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/28422383" @default.
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