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• W2607029394 abstract "Abstract Pure phase monoclinic nano-crystalline Li2TiO3 powder was synthesized by a novel urea assisted solid state synthesis method using readily available and economical precursors. A single phase and well crystalline Li2TiO3 powder has been obtained at slightly lower temperature (600–700 °C) and shorter duration (2 h) as compared to the conventional solid state method. The proposed method has significant advantages in comparison to other viable methods mainly in terms of phase purity, powder properties and sinterability. Analysis of chemical composition using inductively coupled plasma atomic emission spectroscopy (ICP-AES) shows no loss of lithium from Li2TiO3 in the proposed method. The emergence of monoclinic Li2TiO3 phase was confirmed by X-ray diffraction (XRD) pattern of as-synthesized powder. The crystallite size of Li2TiO3 powder was calculated to be in the range of 15–80 nm, which varied as a function of urea composition and temperature. The morphology of as-prepared Li2TiO3 powders was examined by scanning electron microscope (SEM). The effect of urea composition on phase and morphology was investigated so as to delineate the role of urea. Upon sintering at" @default.
• W2607029394 created "2017-04-28" @default.
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• W2607029394 date "2017-07-01" @default.
• W2607029394 modified "2023-09-23" @default.
• W2607029394 title "Monoclinic β-Li 2 TiO 3 nanocrystalline particles employing novel urea assisted solid state route: Synthesis, characterization and sintering behavior" @default.
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• W2607029394 doi "https://doi.org/10.1016/j.jnucmat.2017.04.022" @default.
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