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- W2607301274 abstract "1) Reaction of 4-nitropyridine N-oxide with phosphorus trichloride in chloroform results in the formation of N-(4′-pyridyl)-4-pyridone by the secondary reaction of 4-nitropyridine and phosphoryl chloride formed by the first reaction.2) 4-Nitropyridine undergoes similar decomposition when allowed to stand with thionyl, sulfuryl or acetyl chloride, or warmed with these reagents in chloroform.3) 4-Nitropyridine undergoes similar decomposition to N-(4′-pyridyl)-4-pyridone by a long standing by itself.4) Heating this N-(4′-pyridyl)-4-pyridone with phosphoryl chloride in a sealed tube to 120-130° results in the formation of approximately two moles of 4-chloropyridine." @default.
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- W2607301274 date "1952-01-01" @default.
- W2607301274 modified "2023-10-03" @default.
- W2607301274 title "Decomposition of 4-Nitropyridine" @default.
- W2607301274 doi "https://doi.org/10.1248/yakushi1947.72.8_1051" @default.
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