Matches in SemOpenAlex for { <https://semopenalex.org/work/W2608339820> ?p ?o ?g. }
Showing items 1 to 84 of
84
with 100 items per page.
- W2608339820 abstract "Abstract A simple and efficient method to prepare 1-(1-chlorocyclopropyl)-2-(1,2,4-triazol-1-yl)ethan-1-one via nucleophilic substitution of 2-chloro-1-(1-chlorocyclopropyl)ethanone and 1,2,4-triazole is described. The title compound is the key intermediate required for the synthesis of prothioconazole, a promising agricultural fungicide. By exploring changes in the reaction time, temperature, ratio of starting reagents, acid binding agent, and the nature of phase transfer catalyst, the reaction conditions could be optimized to afford the desired N-alkylated material in near-quantitative yield. The ultimate yield of the product after recrystallization was 93%, with a purity of 99% based on its characterization by Gas Chromatography-Mass Spectrometer (GC-MS), Fourier Transform infrared spectroscopy (IR), Proton Magnetic Resonance ( 1 H NMR), and Carbon-13 Nuclear Magnetic Resonance ( 13 C NMR). The synthetic process is suitable for industrial application, with the advantages of high yield and facile preparation under mild operating conditions." @default.
- W2608339820 created "2017-05-05" @default.
- W2608339820 creator A5034216326 @default.
- W2608339820 creator A5037349401 @default.
- W2608339820 creator A5040536826 @default.
- W2608339820 creator A5070187113 @default.
- W2608339820 creator A5080733479 @default.
- W2608339820 date "2017-03-28" @default.
- W2608339820 modified "2023-09-26" @default.
- W2608339820 title "Synthesis and Characterization of 1-(1-chlorocyclopropyl)-2-(1,2,4-triazol-1-yl)ethan-1-one" @default.
- W2608339820 cites W1980760549 @default.
- W2608339820 cites W1988624158 @default.
- W2608339820 cites W2051874370 @default.
- W2608339820 cites W2093065499 @default.
- W2608339820 cites W2132013414 @default.
- W2608339820 doi "https://doi.org/10.1515/pjct-2017-0006" @default.
- W2608339820 hasPublicationYear "2017" @default.
- W2608339820 type Work @default.
- W2608339820 sameAs 2608339820 @default.
- W2608339820 citedByCount "1" @default.
- W2608339820 countsByYear W26083398202018 @default.
- W2608339820 crossrefType "journal-article" @default.
- W2608339820 hasAuthorship W2608339820A5034216326 @default.
- W2608339820 hasAuthorship W2608339820A5037349401 @default.
- W2608339820 hasAuthorship W2608339820A5040536826 @default.
- W2608339820 hasAuthorship W2608339820A5070187113 @default.
- W2608339820 hasAuthorship W2608339820A5080733479 @default.
- W2608339820 hasBestOaLocation W26083398201 @default.
- W2608339820 hasConcept C103319777 @default.
- W2608339820 hasConcept C127413603 @default.
- W2608339820 hasConcept C134121241 @default.
- W2608339820 hasConcept C135731615 @default.
- W2608339820 hasConcept C13965031 @default.
- W2608339820 hasConcept C151730666 @default.
- W2608339820 hasConcept C160892712 @default.
- W2608339820 hasConcept C161790260 @default.
- W2608339820 hasConcept C163111631 @default.
- W2608339820 hasConcept C164361826 @default.
- W2608339820 hasConcept C178790620 @default.
- W2608339820 hasConcept C178907741 @default.
- W2608339820 hasConcept C185592680 @default.
- W2608339820 hasConcept C191897082 @default.
- W2608339820 hasConcept C192562407 @default.
- W2608339820 hasConcept C195702682 @default.
- W2608339820 hasConcept C40875361 @default.
- W2608339820 hasConcept C42360764 @default.
- W2608339820 hasConcept C86803240 @default.
- W2608339820 hasConceptScore W2608339820C103319777 @default.
- W2608339820 hasConceptScore W2608339820C127413603 @default.
- W2608339820 hasConceptScore W2608339820C134121241 @default.
- W2608339820 hasConceptScore W2608339820C135731615 @default.
- W2608339820 hasConceptScore W2608339820C13965031 @default.
- W2608339820 hasConceptScore W2608339820C151730666 @default.
- W2608339820 hasConceptScore W2608339820C160892712 @default.
- W2608339820 hasConceptScore W2608339820C161790260 @default.
- W2608339820 hasConceptScore W2608339820C163111631 @default.
- W2608339820 hasConceptScore W2608339820C164361826 @default.
- W2608339820 hasConceptScore W2608339820C178790620 @default.
- W2608339820 hasConceptScore W2608339820C178907741 @default.
- W2608339820 hasConceptScore W2608339820C185592680 @default.
- W2608339820 hasConceptScore W2608339820C191897082 @default.
- W2608339820 hasConceptScore W2608339820C192562407 @default.
- W2608339820 hasConceptScore W2608339820C195702682 @default.
- W2608339820 hasConceptScore W2608339820C40875361 @default.
- W2608339820 hasConceptScore W2608339820C42360764 @default.
- W2608339820 hasConceptScore W2608339820C86803240 @default.
- W2608339820 hasLocation W26083398201 @default.
- W2608339820 hasLocation W26083398202 @default.
- W2608339820 hasOpenAccess W2608339820 @default.
- W2608339820 hasPrimaryLocation W26083398201 @default.
- W2608339820 hasRelatedWork W1561108185 @default.
- W2608339820 hasRelatedWork W2021379719 @default.
- W2608339820 hasRelatedWork W2021939235 @default.
- W2608339820 hasRelatedWork W2110618058 @default.
- W2608339820 hasRelatedWork W2372525292 @default.
- W2608339820 hasRelatedWork W2392834918 @default.
- W2608339820 hasRelatedWork W2952076161 @default.
- W2608339820 hasRelatedWork W2976128481 @default.
- W2608339820 hasRelatedWork W4206458270 @default.
- W2608339820 hasRelatedWork W4295868812 @default.
- W2608339820 isParatext "false" @default.
- W2608339820 isRetracted "false" @default.
- W2608339820 magId "2608339820" @default.
- W2608339820 workType "article" @default.