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- W2610048453 abstract "1,3-Bis(5-methyl-2-thiazolylimino) isoindoline derivative (EDOT-BTI) containing an electropolymerizable group is prepared using the Linstead method. According to this two-step method phthalonitrile derivative EDOT-Pht is converted to 1,3-diiminoisoindoline EDOT-DII first then EDOT-DII is reacted with 2-amino-5-methylthiazole in ethanol during 5 day reflux. Palladium(II) complex (EDOT-PdBTI) of EDOT-BTI is synthesized in benzene using [Pd(PhCN)2Cl2] as the palladium(II) precursor and triethylamine as auxiliary base. In order to show the H2O2 sensing properties of EDOT-PdBTI, electrochemical characterizations of EDOT-BTI and EDOT-PdBTI are performed and then modified glassy carbon electrode is constructed with electropolymerization of EDOT-PdBTI. GCE/PEDOT-PdBTI shows a wave at 0.215 V. With increasing H2O2 concentration, this wave shifts to −0.075 V. A linear range is observed between 0.72 and 13.6 μmol dm−3 with a limit of detection of 0.21 μmoldm−3 and sensitivity of 0.0153 mV μmol−1 dm−3. These data illustrate possible use of the electrode as a potentiometric H2O2 sensor." @default.
- W2610048453 created "2017-05-05" @default.
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- W2610048453 date "2017-05-05" @default.
- W2610048453 modified "2023-10-10" @default.
- W2610048453 title "Synthesis and electropolymerization of EDOT modified 1,3-bis(5-methyl-2-thiazolylimino)isoindolinato palladium(II) complex for electrochemical detection of hydrogen peroxide" @default.
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- W2610048453 doi "https://doi.org/10.1080/00958972.2017.1322695" @default.
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