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• W2610148458 abstract "Restricted by their molecular structure defects, poly(methylphenylsiloxanes) usually exhibit a relatively low thermal stability, thus limiting their application in high-temperature areas. In this paper, we introduce a cost-effective synthesis method to prepare poly(methylphenylsiloxanes) (PPMS-M) with methyl–phenyl mixed cyclic monomers as raw materials. The molecular structure characterization shows that PPMS-M contain abundant phenyl groups, and the phenylsiloxane units are evenly distributed among methylsiloxane segments. The thermal degradation kinetics are systematically studied with the Flynn–Wall–Ozawa method. It shows that PPMS-M exhibits much higher degradation activation energy than ordinary poly(methylphenylsiloxanes) (PPMS-PD) does, which is prepared by 2,4,6-trimethyl-2,4,6-triphenylcyclotrisiloxane (P3) and octamethylcyclotetrasiloxane (D4). The thermogravimetry–Fourier transform infrared characterization shows that the degradation process of the phenyl group in PPMS-M occurs at temperatures of 100–200 °C higher than those for PPMS-PD. PPMS-M exhibits good thermal stability and a low glass transition temperature. Our method would be applied to cost-effective synthesis of other high-performance functional polysiloxanes." @default.
• W2610148458 created "2017-05-05" @default.
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• W2610148458 date "2017-06-19" @default.
• W2610148458 modified "2023-10-17" @default.
• W2610148458 title "Ring-Opening Copolymerization of Mixed Cyclic Monomers: A Facile, Versatile and Structure-Controllable Approach to Preparing Poly(methylphenylsiloxane) with Enhanced Thermal Stability" @default.
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• W2610148458 doi "https://doi.org/10.1021/acs.iecr.7b01279" @default.
• W2610148458 hasPublicationYear "2017" @default.
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