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- W2610842001 abstract "Phosphorus clusters P-n (n = 1-89) are easily formed from redphosphorus by laser desorption ionization (LDI) and they covera range of up to approx. m/z 3000 in both positive and negativeion mode. The clusters are singly charged and the spectra aresimple because phosphorus is monoisotopic. The mass spectra canbe measured with an acceptable resolution and intensity. Theuse of positively charged P-n clusters for calibration in massspectrometry was examined and it was demonstrated that inexternal calibration a standard deviation of +/-0.04 m/z unitscan be achieved even when using a common commercialmatrix-assisted laser desorption/ionization time-of-flight(MALDI-TOF) instrument. When used as internal standards the P-nclusters react with some analytes - C-60 and C-70 fullerenesand cucurbituril[8], for example. It was also found that redphosphorus is a suitable MALDI matrix for peptides andproteins, illustrated by the examples of a Calmix mixture ofbradykinin, angiotensin, renin, adrenocorticotropic hormoneACTH fragment 18-359 and insulin, and of insulin alone." @default.
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- W2610842001 date "2009-04-06" @default.
- W2610842001 modified "2023-09-24" @default.
- W2610842001 title "Laser desorption ionization of red phosphorus clusters andtheir use for mass calibration in time-of-flight mass" @default.
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