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- W2611052016 abstract "In the presence of iron pentacarbonyl, photochemical reaction between phenylisocyanate and ferrocenylacetylene results in ferrapyrrolinone complex [Fe 2 (CO) 6 (μ 2 ‐η 3 ‐FcC═C(H)C(O)NPh)] ( 1 ) and maleimide 3‐ferrocenyl‐1‐phenyl‐1 H ‐pyrrole‐2,5‐dione ( 2 ). Under similar experimental conditions, ferrocenyl−/phenyl‐substituted butadiyne primarily shows the activation of only one C☰C bond and results in ferrapyrrolinone complexes [Fe 2 (CO) 6 (μ 2 ‐η 3 ‐FcC═C(C☰CR)C(O)NPh)] ( 3 , R = Fc; 3a , R = Ph), maleimides 3‐ferrocenyl‐1‐phenyl‐4‐(ferrocenylethynyl)‐1 H –pyrrole‐2,5‐dione ( 5 ) and 3‐ferrocenyl‐1‐phenyl‐4‐(phenylethynyl)‐1 H –pyrrole‐2,5‐dione ( 5a ) and [Fe 2 (CO) 6 (μ 2 ‐η 3 ‐FcC═C(R)C(O)NPh)] ( 4 ; R = 3‐ferrocenyl‐1‐phenyl‐1 H ‐pyrrole‐2,5‐dione). Compound 4 consists of ferrapyrrolinone and a maleimide unit, formed by the activation of both C☰C bonds of diferrocenylbutadiyne. Activation of both C☰C bonds in a substituted butadiyne is a rare observation. Formation of the ferrapyrrolinone compounds is an advance over the earlier reported methods which generally use internal alkynes and involve prior synthesis of other clusters." @default.
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- W2611052016 date "2017-05-05" @default.
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- W2611052016 title "A photochemical route to ferrocenyl‐substituted ferrapyrrolinone complexes" @default.
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- W2611052016 doi "https://doi.org/10.1002/aoc.3805" @default.
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