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• W2614386557 abstract "A novel and facile strategy is introduced for the preparation of ethylenediaminetetraacetic acid (EDTA) capped magnetite nanoparticles (MNPs). In this strategy, Fe3O4 nanoparticles were electrodeposited from a deposition bath containing 0.005 M Fe2+/Fe3+ nitrate and chlorides alts and 1 g/L EDTA. A simple deposition mode i.e. constant current and two-electrode set-up was used in the electro-synthesis procedure. The magnetite phase of the deposited nanoparticles was confirmed through XRD and FT-IR analyses. Morphological observations through FE-SEM and TEM confirmed the formation of spherical MNP particles with an average size of 10 nm. The EDTA layer on the surface of the electro-synthesized magnetite nanoparticles was proved based on FT-IR, DLS and TG data. Vibrating sample magnetometer (VSM) measurements confirmed the EDTA capped iron oxide nanoparticles to have a super-paramagnetic nature, since they exhibit a high saturation magnetization (Ms = 51.9 emu g−1), as well as, negligible remnant magnetization (Mr = 0.59 emu g−1) and coercivity (Hc = 0.85 Oe). Based on the obtained results, the proposed platform can be considered as a fast, simple and efficient method for the preparation of the EDTA capped magnetite nanoparticles." @default.
• W2614386557 created "2017-05-26" @default.
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• W2614386557 date "2017-10-01" @default.
• W2614386557 modified "2023-09-26" @default.
• W2614386557 title "Ethylenediaminetetraacetic acid capped superparamagnetic iron oxide (Fe 3 O 4 ) nanoparticles: A novel preparation method and characterization" @default.
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• W2614386557 doi "https://doi.org/10.1016/j.jmmm.2017.05.042" @default.
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