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- W2614405480 abstract "Nano plated and high-purity boron carbide (B4C) powder was synthesized via a novel method, based on a solid-state reaction of poly (vinyl alcohol) PVA and boric acid at (200–250) °C in air. The cross-linking between PVA and boric acid was proven by FTIR analysis. The obtained product, a new-type of poly vinyl borate (PVBO), was consecutively pyrolyzed at (700–800) °C for 120 min in air (S1); or was ground and heat treated at 250 °C for 120 min, followed by pyrolysis at (700–800) °C for 120 min in air (S2). Both pyrolyzed specimens (S1& S2) were then heat treated at (1375–1475) °C in an Ar flow for (180-120) min, respectively. XRD analysis shows that high purity B4C was obtained from S2 which was pyrolyzed at 750 °C and heat treated at 1475 °C. Compared to previous methods (commercial or sol-gel etc.), this approach is cost-effective, highly promising, and established a new reaction route in the field of polymer- derived ceramic (PDC)." @default.
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- W2614405480 date "2017-09-01" @default.
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- W2614405480 title "A Novel method of synthesis of high purity nano plated boron carbide powder by a solid-state reaction of poly (vinyl alcohol) and boric acid" @default.
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- W2614405480 doi "https://doi.org/10.1016/j.ceramint.2017.05.120" @default.
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