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- W2615584935 abstract "Electrode reaction mechanisms of electrolytical coating bymetals of paraffin impregnated graphite electrode (PIGE) wereinvestigated by voltamperometric methods including theelimination voltammetry with linear scan (EVLS). The EVLS isbased on the fact that the total voltammetric current (LSV)response consists of a set of particular currents, e.g.charging, diffusion, and kinetic currents having differentdependences on scan rate. From voltammetric currents measuredat different scan rates the elimination procedure enablesselected current components to be eliminated, some currentcomponents to be conserved and unknown processes to be revealed[1-3]. In aqueous acidic solutions one of these processes isthe hydrogen evolution [3,4]. The attention was focused on theinterpretation of electrochemical behavior of metals (Cd, Ni,Co, and Cu) from chloride and sulphate electrolytes.Experiments were performed using the AUTOLAB potentiostat(EcoChemie) with three-electrode setting. For the calculationof elimination functions three voltammetric curves at differentscan rates were recorded under the same experimental conditions(potential step and range) [5]. The differences in mechanismsof metals deposition from various supporting electrolytes havebeen observed as a function of metal concentrations, pH, scanrate, and electrode surface roughness. The EVLS helped also toidentify the charge carrying species of metals, and the effectof electrode surface roughness. During the deposition processesthe EVLS (E4 function) revealed the pre-peak (Ipp) reflectingsome kinetically controlled surface reactions (e.g. adsorption,surface diffusion, nucleation). The study showed that the EVLSis suitable and powerful tool for the study of reductionprocesses of metals not only on mercury electrodes but also onsolid electrodes." @default.
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- W2615584935 date "2006-01-01" @default.
- W2615584935 modified "2023-09-26" @default.
- W2615584935 title "Elimination voltammetry as a powerful tool for the study ofelectrodeposition of metals" @default.
- W2615584935 hasPublicationYear "2006" @default.
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