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- W2616453306 abstract "Complex uranyl fluorides of the general formulae BH2[UO2F4]·nH2O, MII[UO2F4]·nH2O and M2I[UO2F4]·nH2O where B = organic diamine base, viz. biguanide and phenyl biguanide, MII = Ba2+ and bivalent complex cations [Ni(py)4]2+ [Ni(en)2]2+ and M1 = alkali metals Na+, K+ and NH4+ have been isolated in pure state. The compounds with organic bases were obtained by mixing the organic base fluorides with uranyl fluoride in 20% HF medium. The compounds with complex cations were obtained by the action of pyridine or ethylene diamine on a mixture of nickel fluoride and uranyl fluoride. The Na+, K+ and NH4+ salts were obtained by the metathesis of the compounds containing complex cations with NaClO4, KI and NH4I respectively. The barium salt was obtained by the metathesis between the potassium salt and BaCl2 in the presence of boric acid. The solubilities of some of the salts in water have been determined. The salts have been characterised by elemental analysis, metathesis studies, conductivity measurement, thermogravimetric analysis and i.r. spectral studies." @default.
- W2616453306 created "2017-05-26" @default.
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- W2616453306 date "1971-08-01" @default.
- W2616453306 modified "2023-09-27" @default.
- W2616453306 title "Fluoro complexes of hexavalent uranium—III" @default.
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- W2616453306 doi "https://doi.org/10.1016/0022-1902(71)80231-2" @default.
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