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• W2616461488 abstract "n ‐Dodecyltriethoxysilane (DTEOS) modified NaHSO 4 /MCM‐41 catalysts (silanized catalysts) were synthesized by different impregnation sequences and evaluated in the liquid‐phase dehydration of castor oil. The samples were evaluated by X‐ray diffraction, nitrogen adsorption‐desorption, SEM, TEM, FT‐IR spectroscopy, XPS, 29 Si MAS NMR spectroscopy, contact angle measurements, NH 3 ‐TPD, and pyridine‐FT‐IR spectroscopy. The analyses demonstrated that silanization enhanced the hydrophobicity of the catalysts, and the impregnation sequence of silanized catalysts had a significant effect on the NaHSO 4 dispersion, surface area, acid distribution, and hydrophobicity of the silanized catalysts. The catalytic activity of the silanized catalysts was much higher than that of NaHSO 4 /MCM‐41. Among the silanized catalysts, the catalyst prepared by simultaneous impregnation with DTEOS and NaHSO 4 showed the highest iodine value of 141.8 [g(I 2 ) per 100 g] and lowest hydroxyl value of 11.3 [mg(KOH) · g –1 ]." @default.
• W2616461488 created "2017-05-26" @default.
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• W2616461488 date "2017-05-19" @default.
• W2616461488 modified "2023-10-18" @default.
• W2616461488 title "Dehydration of Castor Oil over NaHSO₄ /MCM-41 Catalyst Modified by <i>n</i> -Dodecyltriethoxysilane" @default.
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• W2616461488 doi "https://doi.org/10.1002/zaac.201700066" @default.
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