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- W2616727965 abstract "Pd(MeCN)2Cl2 enables the α-stereoselective catalytic synthesis of 2,3-unsaturated O-glycosides from O(3)-acylated glycals without the requirement for additives to preactivate either donor or nucleophile. Mechanistic studies suggest that, unlike traditional (η3-allyl)palladium-mediated processes, the reaction proceeds via an alkoxy-palladium intermediate that increases the proton acidity and oxygen nucleophilicity of the alcohol. The method is exemplified with the synthesis of a range of glycosides and glycoconjugates of synthetic utility." @default.
- W2616727965 created "2017-05-26" @default.
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- W2616727965 date "2017-05-17" @default.
- W2616727965 modified "2023-10-16" @default.
- W2616727965 title "Palladium-Catalyzed α-Stereoselective <i>O</i>-Glycosylation of O(3)-Acylated Glycals" @default.
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- W2616727965 doi "https://doi.org/10.1021/acs.orglett.7b01092" @default.
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