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• W2616915691 abstract "Continuous hydrothermal synthesis (CHS) of nanoparticles is most commonly associated with the production of metal oxides and ceramics. However, recent work has demonstrated that layered double hydroxides (LDH) can also be synthesised via this method. This research investigates how altering temperature, pressure and precursor base concentration affects growth and nucleation rates which impact on LDH characteristics. Experiments examined the separate effects of increased temperature, pressure and NaOH concentration on crystal domain length (CDL) and surface area. Adjustments to temperature and pressure in the reactor system resulted in variations in CDL. High temperature (200 °C) with increasing pressure resulted in an increase in CDL between 50 bar and 100 bar, then a decrease up to 200 bar. Crystal domain length of samples synthesised at 75 °C and 150 °C showed increases between 50 bar and 150 bar but a decrease at higher pressure. Variation in CDL showed little impact on specific surface area (4-7 m2 g−1). Increasing NaOH decreased CDL. High precursor NaOH causes rapid nucleation to occur to the detriment of crystal growth. Samples with 1 M and 0.5 M NaOH exhibit Ca(OH)2 impurities as the increased NaOH causes precipitation of Ca2+." @default.
• W2616915691 created "2017-06-05" @default.
• W2616915691 creator A5057905796 @default.
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• W2616915691 date "2017-10-01" @default.
• W2616915691 modified "2023-10-16" @default.
• W2616915691 title "Continuous hydrothermal synthesis of Ca2Al-NO3 layered double hydroxides: The impact of reactor temperature, pressure and NaOH concentration on crystal characteristics" @default.
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• W2616915691 doi "https://doi.org/10.1016/j.jcis.2017.05.105" @default.
• W2616915691 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/28605712" @default.
• W2616915691 hasPublicationYear "2017" @default.
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