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- W2617663444 abstract "A new melamine (ME)–barbituric acid (BA) rosette‐type system has been prepared and characterized. The introduction of a pyridyl group on the barbituric acid moiety allows coordination of metal ions at the periphery of the ME 3 · BA 3 rosette. Reactions of 1.5 equiv. of [Ru(cym)Cl 2 ] 2 (cym = p ‐cymene) or [M(Cp*)Cl 2 ] 2 (Cp* = pentamethylcyclopentadienyl; M = Rh, Ir) with the rosette afford the corresponding ME 3 · [BA{Ru(cym)Cl 2 }] 3 and ME 3 · [BA{M(Cp*)Cl 2 }] 3 assemblies. The neutral metal‐containing rosettes ME 3 · [BA{Ru(cym)Cl 2 }] 3 and ME 3 · [BA{Rh(Cp*)Cl 2 }] 3 can also be obtained by adding the mononuclear complexes [BA{Ru(cym)Cl 2 }] and [BA{Rh(Cp*)Cl 2 }] to N , N′ ‐bis(4‐ tert ‐butylphenyl)melamine in chloroform. In addition, the triphenylphosphine derivatives [Ru(cym)(PPh 3 )Cl 2 ] or [M(Cp*)(PPh 3 )Cl 2 ] react with ME 3 · BA 3 in the presence of silver triflate to generate the ionic rosette‐type assemblies ME 3 · [BA{Ru(cym)(PPh 3 )Cl} + ] 3 · 3CF 3 SO 3 – and ME 3 · [BA{M(Cp*)(PPh 3 )Cl} + ] 3 · 3CF 3 SO 3 – , respectively." @default.
- W2617663444 created "2017-06-05" @default.
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- W2617663444 date "2017-07-06" @default.
- W2617663444 modified "2023-09-22" @default.
- W2617663444 title "Coordination of Piano-Stool Complexes to a Hydrogen-Bonded Rosette-Type Assembly" @default.
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- W2617663444 doi "https://doi.org/10.1002/ejic.201700458" @default.
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