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- W2617963991 abstract "Herein, we demonstrate the synthesis of a well-defined diblock copolymer consisting of isotactic polystyrene (iPS) and linear polyethylene, isotactic polystyrene-block-polyethylene (iPS-b-PE), by the combination of sequential monomer addition and hydrogenation. Isospecific living polymerization of styrene and living trans-1,4-polymerization of 1,3-butadiene were catalyzed by 1,4-dithiabutandiyl-2,2′-bis(6-cumenyl-4-methylphenoxy) titanium dichloride (complex 1) activated by triisobutyl aluminum modified methylaluminoxane (MMAO) at room temperature to provide highly isotactic polystyrene (iPS) and 1,4-trans-polybutadiene (1,4-trans-PBD) with narrow molecular weight distribution. Furthermore, the iPS-b-1,4-trans-PBD was synthesized via sequential monomer addition in the presence of complex 1 and MMAO. The hydrogenation of the 1,4-trans-PBD block was promoted by RuCl2(PPh3)3 used as a catalyst to produce iPS-b-PE." @default.
- W2617963991 created "2017-06-05" @default.
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- W2617963991 date "2017-05-26" @default.
- W2617963991 modified "2023-10-09" @default.
- W2617963991 title "Synthesis of isotactic polystyrene-block-polyethylene by the combination of sequential monomer addition and hydrogenation of 1,4-trans-polybutadiene block" @default.
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- W2617963991 doi "https://doi.org/10.1007/s10118-017-1933-6" @default.
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