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- W2626133724 abstract "Electron spin resonance and hyperfine sublevel correlation (HYSCORE) spectroscopy at X- and Q-band frequencies have been employed, in conjunction with X-ray absorption spectroscopy (XAS), to determine the geometric and electronic structure of Zn+ ions in H-ZSM-5 zeolite. Zn+ ions were generated by the direct exposure of dehydrated acid H-ZSM-5 to Zn vapors. The number of Zn+ ions is found to increase substantially upon UV irradiation. A single EPR active species is detected, indicating a single site of adsorption, characterized by the presence of an Al3+ site, as revealed by superhyperfine interactions. The full g (gx = 1.9951, gy = 1.9984, gz = 2.0015) and 27Al |A| (Ax = 2.8, Ay = 2.7, Az = 4.6) MHz tensors were resolved, allowing for a detailed description of the geometric and electronic structure of Zn+ ions stabilized in the cages of H-ZSM-5 zeolite. The dispersion and nuclearity of Zn species formed during the sublimation/irradiation process was assessed by means of XAS spectroscopy, which indicates ..." @default.
- W2626133724 created "2017-06-23" @default.
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- W2626133724 date "2017-06-22" @default.
- W2626133724 modified "2023-10-03" @default.
- W2626133724 title "Electronic and Geometrical Structure of Zn<sup>+</sup> Ions Stabilized in the Porous Structure of Zn-Loaded Zeolite H-ZSM-5: A Multifrequency CW and Pulse EPR Study" @default.
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- W2626133724 doi "https://doi.org/10.1021/acs.jpcc.7b04289" @default.
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